Process Intensification of Emulsion Polymerization Using a Compartment Reactor
Identifieur interne : 000927 ( Main/Exploration ); précédent : 000926; suivant : 000928Process Intensification of Emulsion Polymerization Using a Compartment Reactor
Auteurs : Naoto Ohmura [Japon] ; Takafumi Horie [Japon] ; Norihisa Kumagai [Japon] ; Tatsuyuki Esaki [Japon] ; Takaki Yamazaki [Japon]Source :
- Chemical engineering & technology [ 0930-7516 ] ; 2012.
Descripteurs français
- Pascal (Inist)
English descriptors
- KwdEn :
Abstract
Attempts were made to intensify continuous emulsion polymerization using a compartment reactor consisting of three well-mixing compartments. The goal of this intensification is to obtain a stable and monodisperse particle size as well as high monomer conversion, by controlling the mixing under continuous operation. A two-bladed paddle impeller was used in the first compartment to intensify the dispersibility and reactivity in the aqueous phase, while a rotating disk was used in the third compartment to avoid excessive flocculation of the polymer particles. In the second compartment, a two-bladed turbine impeller or a rotating disk was used. The compartment reactor successfully obtained much higher monomer conversion and also more stable and monodisperse particles than a single continuous stirred-tank reactor. The oscillations of the mean particle size were greatly suppressed by spatially different mixing operations.
Affiliations:
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Le document en format XML
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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Process Intensification of Emulsion Polymerization Using a Compartment Reactor</title>
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<author><name sortKey="Horie, Takafumi" sort="Horie, Takafumi" uniqKey="Horie T" first="Takafumi" last="Horie">Takafumi Horie</name>
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<author><name sortKey="Kumagai, Norihisa" sort="Kumagai, Norihisa" uniqKey="Kumagai N" first="Norihisa" last="Kumagai">Norihisa Kumagai</name>
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<series><title level="j" type="main">Chemical engineering & technology</title>
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<idno type="ISSN">0930-7516</idno>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Chemical reactivity</term>
<term>Continuous stirred tank reactor</term>
<term>Emulsion polymerization</term>
<term>Flocculation</term>
<term>Mixing</term>
<term>Paddle impeller</term>
<term>Particle size</term>
<term>Rotating disk</term>
<term>Turbine impeller</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Polymérisation émulsion</term>
<term>Réacteur parfaitement agité</term>
<term>Mélangeage</term>
<term>Dimension particule</term>
<term>Agitateur pale</term>
<term>Réactivité chimique</term>
<term>Disque tournant</term>
<term>Floculation</term>
<term>Agitateur turbine</term>
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<front><div type="abstract" xml:lang="en">Attempts were made to intensify continuous emulsion polymerization using a compartment reactor consisting of three well-mixing compartments. The goal of this intensification is to obtain a stable and monodisperse particle size as well as high monomer conversion, by controlling the mixing under continuous operation. A two-bladed paddle impeller was used in the first compartment to intensify the dispersibility and reactivity in the aqueous phase, while a rotating disk was used in the third compartment to avoid excessive flocculation of the polymer particles. In the second compartment, a two-bladed turbine impeller or a rotating disk was used. The compartment reactor successfully obtained much higher monomer conversion and also more stable and monodisperse particles than a single continuous stirred-tank reactor. The oscillations of the mean particle size were greatly suppressed by spatially different mixing operations.</div>
</front>
</TEI>
<affiliations><list><country><li>Japon</li>
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<tree><country name="Japon"><noRegion><name sortKey="Ohmura, Naoto" sort="Ohmura, Naoto" uniqKey="Ohmura N" first="Naoto" last="Ohmura">Naoto Ohmura</name>
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<name sortKey="Esaki, Tatsuyuki" sort="Esaki, Tatsuyuki" uniqKey="Esaki T" first="Tatsuyuki" last="Esaki">Tatsuyuki Esaki</name>
<name sortKey="Horie, Takafumi" sort="Horie, Takafumi" uniqKey="Horie T" first="Takafumi" last="Horie">Takafumi Horie</name>
<name sortKey="Kumagai, Norihisa" sort="Kumagai, Norihisa" uniqKey="Kumagai N" first="Norihisa" last="Kumagai">Norihisa Kumagai</name>
<name sortKey="Yamazaki, Takaki" sort="Yamazaki, Takaki" uniqKey="Yamazaki T" first="Takaki" last="Yamazaki">Takaki Yamazaki</name>
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</record>
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